Difference:
F20Checklist
(11 vs. 12)
Revision 12
05 Jul 2011 - Main.MarienaSilvestry
META TOPICPARENT
name="CemAdmin"
Contents
F20 Daily Checklist
Operation Parameters for alignments
Gun tilt (check)
Condensor Stigmation
Check image of FEG Tip
Flatfield Tietz camera
F20 Daily Checklist
Cool microscope cold finger
Insert holder to first stop
Do not insert holder
Open colum valves
check for beam
Start Low Dose and click through systematically to "exposure" mode
Load Lose Dose file you will be using
Operation Parameters for alignments
3850-3950 extraction voltage
Gun Lens 3 (make sure it is gun lens 3 by toggling between 2 and 3.)
50 micron condenser aperture (check white board, for now it's position #2)
spot size 2
Gun tilt (check)
Magnification 10kx
Check exposure time without the small screen
Around 2 sec is appropriate
2 sec exposure means 1 nanoAmp of current
if the exposure time is not close to 2 seconds double check for correct operation parameters
If the operation parameters are correct adjust
Gun Tilt
Location: tune/alignments/gun
Adjust the gun tilt alignment to Trash.findDFdf the brightest spot
After adjusting Gun tilt:
If exposure time is over 2 sec increase the extraction voltage and readjust gun tilt
If exposure time is less than 1.4 sec lower the extraction voltage and readjust gun tilt
Condensor Stigmation
Spot size 2
Magnification 250kx
Condense beam to 30mm size
Press
stigmator
button
select
condensor
Use
multifunction knobs
to make beam round
Check image of FEG Tip
Condense beam to point
Beam may not be round at crossover, this is the image of the FEG tip
5mm circle = 10nm
You want the majority of your beam to fit within the 5mm circle
Flatfield Tietz camera
--
KdDerr
- 10 Oct 2006
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