Difference: FilamentExchange (1 vs. 4)

Revision 427 Jul 2007 - Main.KdDerr

 
META TOPICPARENT name="Jeol1230Instructions"
Contents

Filament Exchange

Determining if the filament is blown

  • You had a beam, but now you do not.
    • You did not move the sample
    • or change any microscope parameters
  • The Beam Current value drops to the filament off value

Removing filament

  • Remove sample
  • Press Gun Vent button - control panel
  • Flip Gun Lift switch to on - control panel
  • Wait for gun to lift (patience)
  • Put on lint free gloves
  • Unscrew outer ring from wehnelt assembly
  • Pull out wehnelt assembly
  • Replace the outer ring into the gun
  • Make sure the o-ring is clean and properly aligned
  • Flip Gun Lift switch to off - control panel
  • Wait for gun to lower (patience)
  • Press Gun Vent button - control panel
Added:
>
>

Examine filament for damage

  • Wear lint free gloves when handling gun parts
  • Unscrew the wehnelt cap from the wehnelt assembly
  • Using a stereo microscope observe the filament for damage and determine its cause
 

Cleaning Whenelt Cap

  • You will need
    • Aluminum Foil
    • Pol polish
    • Mr. Clean (ammonia free)
    • 4 - 250 mL beakers
    • Cotton tipped applicators
    • Ethanol (reagent grade and 200 proof)
Changed:
<
<
  • Polish the
>
>
    • Lint free cloth
Added:
>
>
 
  • Wear lint free gloves when handling gun parts
Added:
>
>
  • Use a cotton tipped applicator and pol polish to clean the contamination from the wehnelt opening
  • Only a small amount of pol polish is necessiary
  • Prevent the pol polish from contaminating the threads
  • Polish until all of the visual contamination is gone
    • Continual additions of pol polish will always result in dirty looking resudue on cotton applicator
  • Remove all visible pol polish witht he cotton applicator
 
Changed:
<
<
>
>
  • Begin sonication steps (each step is a miniumum of 5 minutes)
Added:
>
>
    • first sonication - Mr. Clean and water
    • second sonication - DI water
    • third sonication - reagent ethanol
    • fourth sonication - 200 proof ethanol
  • Dry with a lint free cloth

 
  • If you have the luxury of time
    • Place the Whenelt cap in 100% Micro-90 overnight
    • This eliminates the Pol polish step
Added:
>
>

Centering the filament

  • Wear lint free gloves when handling gun parts
  • Filaments for the 1230 are precentered at the factory
  • Screw on wehnelt cap and remove old filament
  • Observe the new filament under the stereo microscope for defects
  • Insert new filament using guide pins for orientation
  • The following steps are best carried out under a stereo micrscope
  • Make sure the filament is centered with in the wehnelt opening
  • Screw the wehnelt down until the tip of the filament is flush with the whenelt opening
  • Retract the filament tip with two full turns of the whenelt cap
    • Each full turn onthe wehnelt cap is equal to 0.5mm
    • Double check your work by making sure the filament tip disappears when tilted to a 45 degree angle
 
Added:
>
>

Replace the wehnelt assembly into the microscope

  • Press Gun Vent button - control panel
  • Flip Gun Lift switch to on - control panel
  • Wait for gun to lift (patience)
  • Put on lint free gloves
  • Unscrew outer ring from wehnelt assembly
  • Push in wehnelt assembly using the guide pins for orientation
  • Replace the outer ring into the gun
  • Make sure the o-ring is clean and properly aligned
  • Flip Gun Lift switch to off - control panel
  • Wait for gun to lower (patience)
  • Press Gun Vent button - control panel

Essential aligments after filament replacement

  • Gun shift center beam at crossover
  • CL Stig in setup menu/F1/F2
    • Desaturate filament
    • Make filament shadow symetrical
  • Gun tilt
 

  • Set ALLOWTOPICVIEW =

-- KdDerr - 27 Jul 2007

Revision 327 Jul 2007 - Main.KdDerr

 
META TOPICPARENT name="Jeol1230Instructions"
Contents

Filament Exchange

Determining if the filament is blown

  • You had a beam, but now you do not.
    • You did not move the sample
    • or change any microscope parameters
  • The Beam Current value drops to the filament off value

Removing filament

  • Remove sample
  • Press Gun Vent button - control panel
  • Flip Gun Lift switch to on - control panel
  • Wait for gun to lift (patience)
  • Put on lint free gloves
  • Unscrew outer ring from wehnelt assembly
  • Pull out wehnelt assembly
  • Replace the outer ring into the gun
Changed:
<
<
  • Make sure the o-ring in clean and in its groove
>
>
  • Make sure the o-ring is clean and properly aligned
Added:
>
>
  • Flip Gun Lift switch to off - control panel
  • Wait for gun to lower (patience)
  • Press Gun Vent button - control panel

Cleaning Whenelt Cap

  • You will need
    • Aluminum Foil
    • Pol polish
    • Mr. Clean (ammonia free)
    • 4 - 250 mL beakers
    • Cotton tipped applicators
    • Ethanol (reagent grade and 200 proof)
  • Polish the
  • Wear lint free gloves when handling gun parts

  • If you have the luxury of time
    • Place the Whenelt cap in 100% Micro-90 overnight
    • This eliminates the Pol polish step
 

  • Set ALLOWTOPICVIEW =

-- KdDerr - 27 Jul 2007

Revision 227 Jul 2007 - Main.KdDerr

 
META TOPICPARENT name="Jeol1230Instructions"
Contents

Filament Exchange

Determining if the filament is blown

  • You had a beam, but now you do not.
    • You did not move the sample
    • or change any microscope parameters
  • The Beam Current value drops to the filament off value

Removing filament

  • Remove sample
Changed:
<
<
  • Press Gun Vent button on control panel
  • Flip Gun Lift switch to on control panel
>
>
  • Press Gun Vent button - control panel
  • Flip Gun Lift switch to on - control panel
 
  • Wait for gun to lift (patience)
  • Put on lint free gloves
  • Unscrew outer ring from wehnelt assembly
  • Pull out wehnelt assembly
  • Replace the outer ring into the gun
  • Make sure the o-ring in clean and in its groove

  • Set ALLOWTOPICVIEW =

-- KdDerr - 27 Jul 2007

Revision 127 Jul 2007 - Main.KdDerr

 
META TOPICPARENT name="Jeol1230Instructions"
Contents

Filament Exchange

Determining if the filament is blown

  • You had a beam, but now you do not.
    • You did not move the sample
    • or change any microscope parameters
  • The Beam Current value drops to the filament off value

Removing filament

  • Remove sample
  • Press Gun Vent button on control panel
  • Flip Gun Lift switch to on control panel
  • Wait for gun to lift (patience)
  • Put on lint free gloves
  • Unscrew outer ring from wehnelt assembly
  • Pull out wehnelt assembly
  • Replace the outer ring into the gun
  • Make sure the o-ring in clean and in its groove

  • Set ALLOWTOPICVIEW =

-- KdDerr - 27 Jul 2007

 
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